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10.1007/s00216-014-7907-4 http://scihub22266oqcxt.onion/10.1007/s00216-014-7907-4 C4685456!4685456!24948088     free     free     free Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 229.6 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534 Deprecated: Implicit conversion from float 263.2 to int loses precision in C:\Inetpub\vhosts\kidney.de\httpdocs\pget.php on line 534       Anal+Bioanal+Chem 2014 ; 406 (20): 5039-47 Nephropedia Template TP {{tp|p=24948088|t=2014. Measurement of Mercury Species in Human Blood using Triple Spike Isotope Dilution with SPME-GC-ICP-DRC-MS |pdf=|usr=}}{{24948088}} gab.com Text Measurement of Mercury Species in Human Blood using Triple Spike Isotope Dilution with SPME-GC-ICP-DRC-MS JO: Anal Bioanal Chem http://www.kidney.de/pget.php?&tw=1&pmid=24948088 #FOAvip The measurement of different mercury compounds in human blood can provide valuable information about the type of mercury exposure. To this end, our laboratory developed a biomonitoring method for the quantification of inorganic (iHg), methyl (MeHg) and ethyl (EtHg) mercury in whole blood using a triple spike isotope dilution (TSID) quantification method employing capillary gas chromatography (GC) and inductively coupled dynamic reaction cell mass spectrometry (ICP-DRC-MS). We used a robotic CombiPAL® sample handling station featuring twin fiber-based solid phase microextraction (SPME) injector heads. The use of two SPME fibers significantly reduces sample analysis cycle times making this method very suitable for high sample throughput, which is a requirement for large public health biomonitoring studies. Our sample preparation procedure involved solubilization of blood samples with tetramethylammonium hydroxide (TMAH) followed by the derivatization with sodium tetra(n-propyl)borate (NaBPr4) to promote volatility of mercury species. We thoroughly investigated mercury species stability in the blood matrix during the course of sample treatment and analysis. The method accuracy for quantifying iHg, MeHg and EtHg was validated using NIST standard reference materials (SRM 955c Level 3) and the Centre de Toxicologie du Québec (CTQ) proficiency testing (PT) samples. The limit of detection (LOD) for iHg, MeHg and EtHg in human blood was determined to be 0.27, 0.12, and 0.16 ?g/L, respectively. Twit Text FOAVip Measurement of Mercury Species in Human Blood using Triple Spike Isotope Dilution with SPME-GC-ICP-DRC-MS ????Anal Bioanal Chem http://www.kidney.de/pget.php?&tw=1&pmid=24948088 #FOAvip Twit Text # Free Paper on # # # # # LINK http://www.kidney.de/pget.php?&tw=1&pmid=24948088 #FOAvip English Wikipedia <ref>{{Cite pmid|24948088}}</ref> Measurement of Mercury Species in Human Blood using Triple Spike Isotope Dilution with SPME-GC-ICP-DRC-MS #MMPMID24948088 Sommer YL; Verdon CP; Fresquez MR; Ward CD; Wood EB; Pan Y; Caldwell KL; Jones RL Anal Bioanal Chem 2014[Aug]; 406 (20): 5039-47 PMID24948088show ga The measurement of different mercury compounds in human blood can provide valuable information about the type of mercury exposure. To this end, our laboratory developed a biomonitoring method for the quantification of inorganic (iHg), methyl (MeHg) and ethyl (EtHg) mercury in whole blood using a triple spike isotope dilution (TSID) quantification method employing capillary gas chromatography (GC) and inductively coupled dynamic reaction cell mass spectrometry (ICP-DRC-MS). We used a robotic CombiPAL® sample handling station featuring twin fiber-based solid phase microextraction (SPME) injector heads. The use of two SPME fibers significantly reduces sample analysis cycle times making this method very suitable for high sample throughput, which is a requirement for large public health biomonitoring studies. Our sample preparation procedure involved solubilization of blood samples with tetramethylammonium hydroxide (TMAH) followed by the derivatization with sodium tetra(n-propyl)borate (NaBPr4) to promote volatility of mercury species. We thoroughly investigated mercury species stability in the blood matrix during the course of sample treatment and analysis. The method accuracy for quantifying iHg, MeHg and EtHg was validated using NIST standard reference materials (SRM 955c Level 3) and the Centre de Toxicologie du Québec (CTQ) proficiency testing (PT) samples. The limit of detection (LOD) for iHg, MeHg and EtHg in human blood was determined to be 0.27, 0.12, and 0.16 ?g/L, respectively. äMeasurement of Mercury Species in Human Blood using Triple Spike Isoto(epmc).pdf DeepDyve Pubget Overpricing