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10.1007/s00706-013-0978-7

http://scihub22266oqcxt.onion/10.1007/s00706-013-0978-7
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C4495021!4495021!26166887
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suck abstract from ncbi


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pmid26166887      Monatsh+Chem 2014 ; 145 (1): 213-6
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  • Ultrasound-mediated synthesis of N,N-bis(phenacyl)aniline under solvent-free conditions #MMPMID26166887
  • He J; Shi L; Liu S; Jia P; Wang J; Hu R
  • Monatsh Chem 2014[]; 145 (1): 213-6 PMID26166887show ga
  • Abstract: An efficient method for the synthesis of N,N-bis(phenacyl)anilines was developed via smooth condensation of anilines with ?-bromoacetophenones in the presence of sodium carbonate as acid acceptor and polyethylene glycol 400 (PEG 400) as catalyst at room temperature under solvent-free conditions by using 350 W ultrasound irradiation. In addition to experimental simplicity, the main advantages of the procedure are mild conditions, short reaction times (30?45 min), and high yields (73?83 %). Graphical Abstract:
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