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10.1021/acs.orglett.0c02848

http://scihub22266oqcxt.onion/10.1021/acs.orglett.0c02848
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32931286!7536717!32931286
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suck abstract from ncbi


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pmid32931286      Org+Lett 2020 ; 22 (19): 7656-7661
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  • Expanding Access to Remdesivir via an Improved Pyrrolotriazine Synthesis: Supply Centered Synthesis #MMPMID32931286
  • Paymode DJ; Cardoso FSP; Agrawal T; Tomlin JW; Cook DW; Burns JM; Stringham RW; Sieber JD; Gupton BF; Snead DR
  • Org Lett 2020[Oct]; 22 (19): 7656-7661 PMID32931286show ga
  • Pyrrolotriazine 1 is an important precursor to remdesivir. Initial results toward an efficient synthesis are disclosed consisting of sequential cyanation, amination, and triazine formation beginning from pyrrole. This route makes use of highly abundant, commoditized raw material inputs. The yield of triazine was doubled from 31% to 59%, and the synthetic step count was reduced from 4 to 2. These efforts help to secure the remdesivir supply chain.
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