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2018 ; 5
(Pt 2
): 190-199
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Electron crystallography with the EIGER detector
#MMPMID29765609
Tinti G
; Fröjdh E
; van Genderen E
; Gruene T
; Schmitt B
; de Winter DAM
; Weckhuysen BM
; Abrahams JP
IUCrJ
2018[Mar]; 5
(Pt 2
): 190-199
PMID29765609
show ga
Electron crystallography is a discipline that currently attracts much attention
as method for inorganic, organic and macromolecular structure solution. EIGER, a
direct-detection hybrid pixel detector developed at the Paul Scherrer Institut,
Switzerland, has been tested for electron diffraction in a transmission electron
microscope. EIGER features a pixel pitch of 75 × 75 µm(2), frame rates up to
23 kHz and a dead time between frames as low as 3 µs. Cluster size and modulation
transfer functions of the detector at 100, 200 and 300 keV electron energies are
reported and the data quality is demonstrated by structure determination of a
SAPO-34 zeotype from electron diffraction data.